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大学物理实验, 2025, 38(4): 23-27     https://doi.org/10,14139/j.cnki.cn22-1228.2025.04.004
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离心法制作X射线小周期相位光栅
李乔飞1,李青华2,李晨阳3,申小萌1
1.新乡学院 物理与电子工程学院,河南 新乡 453003;2.郑州工程技术学院 机械与电气工程学院,河南 郑州 450000;3.河南科技学院 信息工程学院,河南 新乡 453003
Fabrication of Small-period X-ray Phase Gratings by Centrifugation Method
LI Qiaofei1,LI Qinghua2,LI Chenyang3,SHEN Xiaomeng
1.School of Physics and Electronic Engineering,Xinxiang University,Xinxiang 453003,China;2.School of Mechanical and Electrical Engineering,Zhengzhou University of Technology,Zhengzhou 450000 China;3.School of Information Engineering,Henan Institute of Science and Technology,Xinxiang 453003,China
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摘要 

级联泰伯劳干涉仪由泰伯劳与逆泰伯劳装置级联而成,避免了小周期吸收光栅的制作。根据级联装置的限定条件,得出当自成像条纹周期 210 μm 时,能被探测器直接分辨,可省略分析光栅,只需制作小周期相位光栅即可。对于小周期相位光栅的制作,金属纳米颗粒以溶液作载体填充光栅。通过扫描电子显微镜对比不同改性剂对光栅填充效果,发现油酸与 N-甲基吡咯烷酮相比 OP-10填充光栅效果更均匀致密,但存在颗粒团聚现象,通过调整油酸与 N-甲基吡咯烷酮的浓度发现,当 N-甲基吡咯烷酮与异丙醇以0.25mL ∶100mL 的比例配制的悬浊液辅助填充制作的光栅效果最好。

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李乔飞
李青华
李晨阳
申小萌
关键词:  级联泰伯劳干涉仪  离心法  相位光栅  改性剂  X 射线     
Abstract: 

The cascaded Talbot-Lau interferometer is formed by the serial combination of a Talbot-Lau and an inverse Talbot-Lau device,eliminating the need for fabricating small-period absorption gratings.Based on the constraints of the cascaded setup,it show that when the self-imaging fringe period larger than 210 μm,the detector can directly resolve the fringes,thereby omitting the need for an analyzer grating.Only a small-period phase grating needs to be fabricated.For the fabrication of the small-period phase grating,a metal nanoparticle with a solution as the carrier into the grating grooves.By comparing the effects of different modifiers on grating filling efficiency using scanning electron microscopy,it was found that oleic acid and N-methylpyrrolidone (NMP)provided more uniform and dense filling compared to OP-10,though nanoparticle aggregation was observed.The grating fabricated with the assistance of a suspension prepared by mixing N-methylpyrrolidone and isopropanol in a ratio of 0.25 mL 100 mL demonstrated the optimal performance.

Key words:  cascaded talbot-Lau interferometer    centrifugation method    phase gratings    modifier    X-ray
               出版日期:  2025-08-25      发布日期:  2025-08-25      整期出版日期:  2025-08-25
ZTFLH:  O 647.5  
基金资助: 

河南省科技攻关项目 (222102240071);2023 年河南省高等教育教学改革研究与实践项目 (研究生教育类)(2023SJGLX348Y)

引用本文:    
李乔飞, 李青华, 李晨阳, 申小萌. 离心法制作X射线小周期相位光栅 [J]. 大学物理实验, 2025, 38(4): 23-27.
LI Qiaofe, LI Qinghua, LI Chenyang, SHEN Xiaomeng . Fabrication of Small-period X-ray Phase Gratings by Centrifugation Method . Physical Experiment of College, 2025, 38(4): 23-27.
链接本文:  
https://dawushiyan.jlict.edu.cn/CN/10,14139/j.cnki.cn22-1228.2025.04.004  或          https://dawushiyan.jlict.edu.cn/CN/Y2025/V38/I4/23
[1] 李乔飞, 刘兴晨, 李晨阳, 李坤宇, 申小萌 . 基于纳米颗粒自由沉降技术制作吸收光栅 [J]. 大学物理实验, 2025, 38(3): 57-60.
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